{"id":2312,"date":"2026-06-22T07:30:38","date_gmt":"2026-06-22T07:30:38","guid":{"rendered":"https:\/\/www.thermofisher.com\/blog\/accelerating-science-in-china\/?p=2312"},"modified":"2026-06-22T07:30:39","modified_gmt":"2026-06-22T07:30:39","slug":"food-monitoring-antibiotics-residues-in-meat-and-milk","status":"publish","type":"post","link":"https:\/\/www.thermofisher.cn\/blog\/food-monitoring-antibiotics-residues-in-meat-and-milk\/","title":{"rendered":"\u98df\u54c1\u76d1\u6d4b\uff1a\u8089\u7c7b\u548c\u725b\u5976\u4e2d\u7684\u6297\u751f\u7d20\u6b8b\u7559"},"content":{"rendered":"\n<figure class=\"wp-block-image size-large\"><a href=\"https:\/\/www.thermofisher.cn\/cn\/zh\/home\/communities-social\/socialhub\/blog-subscribe.html?icid=cn-blog-subscribe\"><img loading=\"lazy\" decoding=\"async\" width=\"1024\" height=\"176\" src=\"http:\/\/admin.acceleratingscience.com\/accelerating-science-in-china\/wp-content\/uploads\/sites\/28\/2026\/05\/779-\u00d7-134-3-1024x176.jpg\" alt=\"\" class=\"wp-image-2271\" srcset=\"https:\/\/admin.acceleratingscience.com\/accelerating-science-in-china\/wp-content\/uploads\/sites\/28\/2026\/05\/779-\u00d7-134-3-1024x176.jpg 1024w, https:\/\/admin.acceleratingscience.com\/accelerating-science-in-china\/wp-content\/uploads\/sites\/28\/2026\/05\/779-\u00d7-134-3-300x52.jpg 300w, https:\/\/admin.acceleratingscience.com\/accelerating-science-in-china\/wp-content\/uploads\/sites\/28\/2026\/05\/779-\u00d7-134-3-768x132.jpg 768w, https:\/\/admin.acceleratingscience.com\/accelerating-science-in-china\/wp-content\/uploads\/sites\/28\/2026\/05\/779-\u00d7-134-3-1536x264.jpg 1536w, https:\/\/admin.acceleratingscience.com\/accelerating-science-in-china\/wp-content\/uploads\/sites\/28\/2026\/05\/779-\u00d7-134-3-2048x352.jpg 2048w\" sizes=\"auto, (max-width: 1024px) 100vw, 1024px\" \/><\/a><\/figure>\n\n\n\n<p><span><img loading=\"lazy\" decoding=\"async\" height=\"330\" width=\"221\" style=\"float: left\" src=\"http:\/\/admin.acceleratingscience.com\/wp-content\/uploads\/2015\/01\/isolated_milk_bottle.jpg\">\u517d\u7528\u6297\u751f\u7d20\u80fd\u591f\u6709\u6548\u6cbb\u7597\u548c\u9884\u9632\u591a\u79cd\u7ec6\u83cc\u6027\u75be\u75c5\u3002\u4e0d\u5e78\u7684\u662f\uff0c\u6297\u751f\u7d20\u6b8b\u7559\u53ef\u80fd\u4f1a\u6301\u7eed\u5b58\u5728\u4e8e\u725b\u5976\u548c\u8089\u7c7b\u7b49\u52a8\u7269\u6e90\u6027\u4ea7\u54c1\u4e2d\uff0c\u6700\u7ec8\u5bf9\u6d88\u8d39\u8005\u7684\u5065\u5eb7\u6784\u6210\u98ce\u9669\u3002\u6b64\u5916\uff0c\u6297\u751f\u7d20\u4f7f\u7528\u4e0d\u5f53\u8fd8\u4f1a\u4ea7\u751f\u8010\u836f\u83cc\uff0c\u4ece\u800c\u964d\u4f4e\u836f\u7269\u7684\u6574\u4f53\u7597\u6548\u3002\u4e3a\u4e86\u76d1\u6d4b\u662f\u5426\u7b26\u5408\u4e3a\u4fdd\u969c\u516c\u5171\u5065\u5eb7\u800c\u5236\u5b9a\u7684\u6700\u5927\u6b8b\u7559\u9650\u91cf\uff08MRL\uff09\uff0c\u5fc5\u987b\u91c7\u7528\u7075\u654f\u4e14\u5177\u6709\u9009\u62e9\u6027\u7684\u65b9\u6cd5\u6765\u68c0\u6d4b\u6297\u751f\u7d20\u6b8b\u7559\u3002<\/span><\/p>\n\n\n\n<p>\u7531\u4e8e\u9ad8\u5206\u8fa8\u7387\u8d28\u8c31\uff08HRMS\uff09\u5177\u6709\u5feb\u901f\u3001\u7075\u654f\u548c\u53ef\u9760\u7684\u7279\u70b9\uff0c\u56e0\u6b64\u5b83\u6210\u4e3a\u52a8\u7269\u4ea7\u54c1\u4e2d\u6297\u751f\u7d20\u6b8b\u7559\u5e38\u89c4\u7b5b\u67e5\u7684\u6709\u529b\u5019\u9009\u65b9\u6cd5\u3002\u5c24\u5176\u662f Q Exactive \u5e73\u53f0\uff08\u8d5b\u9ed8\u98de\u4e16\u5c14\u79d1\u6280\uff09\u4e0e\u4ee5\u5f80\u7684 Orbitrap \u8d28\u8c31\u6280\u672f\u76f8\u6bd4\uff0c\u4e3a\u7814\u7a76\u4eba\u5458\u548c\u884c\u4e1a\u4e13\u4e1a\u4eba\u58eb\u63d0\u4f9b\u4e86\u66f4\u9ad8\u7684\u7075\u654f\u5ea6\u548c\u9009\u62e9\u6027\uff0c\u4f7f\u8be5\u65b9\u6cd5\u5728\u5408\u89c4\u6027\u76d1\u6d4b\u65b9\u6848\u4e2d\u5c24\u4e3a\u9002\u7528\u3002<\/p>\n\n\n\n<p>\u6700\u8fd1\uff0cCepurnieks \u7b49\u4eba\u00b9\u62a5\u9053\u4e86\u56db\u6781\u6746-Orbitrap \u8d28\u8c31\u9996\u6b21\u7528\u4e8e\u76d1\u6d4b\u8089\u7c7b\u548c\u725b\u5976\u4e2d 26 \u79cd\u591a\u7c7b\u522b\u6297\u751f\u7d20\u6b8b\u7559\uff08\u5305\u62ec\u78fa\u80fa\u7c7b\u3001\u5927\u73af\u5185\u916f\u7c7b\u3001\u56db\u73af\u7d20\u7c7b\u3001\u9752\u9709\u7d20\u7c7b\u548c\u55b9\u8bfa\u916e\u7c7b\uff09\u7684\u5e94\u7528\u3002\u4e3a\u6b64\uff0c\u4ed6\u4eec\u5bf9\u725b\u5976\u548c\u8089\u7c7b\u6837\u54c1\u8fdb\u884c\u4e86\u7b80\u5355\u63d0\u53d6\uff0c\u968f\u540e\u5728 Q-Exactive \u6df7\u5408\u5e73\u53f0\uff08Thermo Scientific\uff09\u4e0a\u91c7\u7528 UPLC-qOrbitrap MS \u8fdb\u884c\u5206\u6790\u3002\u7814\u7a76\u4eba\u5458\u4f9d\u9760 ThermoXcalibur \u548c TraceFinder \u8f6f\u4ef6\uff08\u5747\u6765\u81ea Thermo Scientific\uff09\u8fdb\u884c\u4eea\u5668\u63a7\u5236\u3001\u539f\u59cb\u6570\u636e\u89e3\u6790\u4ee5\u53ca\u5206\u6790\u7269\u7684\u9776\u5411\u8bc6\u522b\/\u5b9a\u91cf\u3002<\/p>\n\n\n\n<p>\u7814\u7a76\u56e2\u961f\u5c06\u63d0\u53d6\u540e\u7684\u6837\u54c1\u5408\u5e76\u4e3a\u4e00\u6b21\u8fdb\u6837\uff0c\u4ece\u800c\u80fd\u591f\u5728\u4e00\u6b21 10 \u5206\u949f\u7684\u8fd0\u884c\u4e2d\u5b8c\u6210\u591a\u7c7b\u522b\u5206\u6790\u3002\u7531\u4e8e\u76d1\u6d4b\u6700\u5927\u6b8b\u7559\u9650\u91cf\uff08MRL\uff09\u7684\u76d1\u7ba1\u65b9\u6848\u8981\u6c42\u4f7f\u7528\u4e24\u4e2a\u79bb\u5b50\u8fdb\u884c\u786e\u8ba4\u00b2\uff0c\u7814\u7a76\u4eba\u5458\u91c7\u7528\u4e86\u5176\u65b9\u6cd5\u7684\u6539\u8fdb\u7248\u672c\uff0c\u5229\u7528\u6570\u636e\u4f9d\u8d56\u578b\u4e32\u8054\u8d28\u8c31\u83b7\u53d6\u5b50\u79bb\u5b50\u8c31\u3002\u4ed6\u4eec\u8fd8\u6307\u51fa\uff0c\u7531\u4e8e\u9488\u5bf9\u8fd9\u7c7b\u79cd\u7c7b\u7e41\u591a\u7684\u5206\u6790\u7269\uff0c\u5e02\u552e\u6807\u8bb0\u5185\u6807\u83b7\u53d6\u6709\u9650\uff0c\u56e0\u6b64\u5176\u5b9a\u91cf\u65b9\u6848\u4f9d\u8d56\u4e8e\u5916\u6807\u6cd5\u548c\u57fa\u8d28\u5339\u914d\u6821\u51c6\u3002<\/p>\n\n\n\n<p>Cepurnieks \u7b49\u4eba\u5728\u6b27\u76df\u89c4\u5b9a\u7684 MRL \u7684 50% \u6c34\u5e73\u4e0b\uff0c\u7528\u65f6\u4e09\u5929\u5bf9\u8be5\u65b9\u6cd5\u5728\u4e24\u79cd\u57fa\u8d28\u4e2d\u8fdb\u884c\u4e86\u9a8c\u8bc1\u3002\u00b3\u4ed6\u4eec\u6bcf\u5929\u4f7f\u7528 20 \u4efd\u5e73\u884c\u6837\u54c1\uff0c\u5728\u6574\u4e2a\u9a8c\u8bc1\u671f\u95f4\u5171\u5206\u6790\u4e86 120 \u4efd\u6837\u54c1\u3002\u5e73\u5747\u56de\u6536\u7387\u5728 83% \u5230 112% \u4e4b\u95f4\u3002\u53d8\u5f02\u7cfb\u6570\u8303\u56f4\u4e3a 8.9% \u5230 39%\u3002\u7814\u7a76\u56e2\u961f\u8ba4\u5b9a\uff0c\u8be5\u65b9\u6cd5\u80fd\u591f\u5728\u4f4e\u4e8e MRL \u7684\u6c34\u5e73\u4e0b\u68c0\u6d4b\u725b\u5976\u548c\u8089\u7c7b\u4e2d\u7684\u6297\u751f\u7d20\u6b8b\u7559\u3002\u4ed6\u4eec\u6307\u51fa\uff0c\u90e8\u5206\u9752\u9709\u7d20\u7c7b\u836f\u7269\uff08\u963f\u83ab\u897f\u6797\u3001\u9752\u9709\u7d20 G\uff09\u8868\u73b0\u51fa\u8f83\u4f4e\u56de\u6536\u7387\uff0c\u56e0\u6b64\u9700\u8981\u6392\u9664\uff0c\u5e76\u5efa\u8bae\u9488\u5bf9\u8fd9\u7c7b\u6297\u751f\u7d20\u91c7\u7528\u5355\u72ec\u7684\u63d0\u53d6\u548c\u5206\u79bb\u65b9\u6848\u3002\u6b64\u5916\uff0c\u4ed6\u4eec\u8868\u793a\uff0c\u8fd9\u79cd UPLC-qOrbitrap \u6280\u672f\u5177\u6709\u4e00\u5b9a\u7684\u7075\u654f\u5ea6\uff0c\u53ef\u5728\u8fd9\u4e9b\u57fa\u8d28\u4e2d\u68c0\u6d4b\u4f4e\u81f3 MRL 5% \u7684\u6b8b\u7559\u3002<\/p>\n\n\n\n<p>\u5f53\u7814\u7a76\u4eba\u5458\u5c06\u8be5\u65b9\u6cd5\u5e94\u7528\u4e8e\u62c9\u8131\u7ef4\u4e9a\u56fd\u5bb6\u6b8b\u7559\u76d1\u6d4b\u8ba1\u5212\u4e2d\u7684 145 \u4efd\u8089\u7c7b\u548c\u725b\u5976\u6837\u54c1\u65f6\uff0c\u4ed6\u4eec\u672a\u53d1\u73b0\u4efb\u4f55\u6837\u54c1\u4e2d\u7684\u6297\u751f\u7d20\u6b8b\u7559\u9ad8\u4e8e\u7ecf\u9a8c\u8bc1\u7684 MRL 50% \u6c34\u5e73\u3002\u603b\u4f53\u800c\u8a00\uff0c\u4ed6\u4eec\u8ba4\u4e3a\u8be5\u65b9\u6cd5\u9002\u7528\u4e8e\u52a8\u7269\u4ea7\u54c1\u4e2d\u6297\u751f\u7d20\u6b8b\u7559\u7684\u5e38\u89c4\u76d1\u6d4b\uff0c\u4e14\u7b26\u5408\u672c\u7814\u7a76\u6240\u5f15\u7528\u7684\u6307\u5357\u3002<\/p>\n\n\n\n<p><span><br><strong><strong>\u53c2\u8003\u6587\u732e<\/strong><\/strong><br><br><\/span>1 Cepurnieks, G. et al. (2015) \u2018<a href=\"http:\/\/www.ncbi.nlm.nih.gov\/pubmed\/25282600\" target=\"_blank\">The development and validation of a rapid method for the&nbsp;determination of antimicrobial agent residues in milk and meat using ultra performance liquid chromatography coupled to quadrupole \u2013Orbitrap mass spectrometry<\/a>.\u2019 Journal of Pharmaceutical and Biomedical Analysis, 102: 184\u2013192. <a href=\"http:\/\/dx.doi.org\/10.1016\/j.jpba.2014.09.005\">http:\/\/dx.doi.org\/10.1016\/j.jpba.2014.09.005<\/a><\/p>\n\n\n\n<p>2 Commission Decision 2002\/657\/EC, Official Journal of the European Communities L221\/8 (2002).<\/p>\n\n\n\n<p><span><span>3 Commission Regulation (EC) 37\/2010, Official Journal of the European Communities L15 (2010).<\/span><\/span><\/p>\n\n\n<script type=\"text\/javascript\">\n\/* <![CDATA[ *\/\nvar 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