Material Analysis by Multi-modal Techniques

Multi-modal techniques mean more from one measurement

Historically, if an analysis required information about the chemical and structural qualities of a material, sequential measurements would be necessary; one measurement for chemical data and another for structural data. However, this sequential data failed to show the true correlation among these qualities, providing poor conclusions and results.

 

Multi-modal techniques allow the user to see how changes in one material quality affect other material qualities, thereby eliminating the guesswork that comes from sequential measurements.

 

Thermo Fisher Scientific offers solutions that help enable materials scientists and engineers to innovate at a faster pace, produce more reliable and better performing materials and processes, reduce costs, and shorten the time to discoveries. Explore how multi-modal techniques can replace sequential measurements.

Nexsa G2 Surface Analysis System

The Thermo Scientific Nexsa G2 X-Ray Photoelectron Spectrometer (XPS) System offers fully automated, high-throughput surface analysis, delivering the data to advance research and development or to solve production problems. By integrating XPS with ion scattering spectroscopy (ISS), UV photoelectron spectroscopy (UPS), reflected electron energy loss spectroscopy (REELS), and Raman spectroscopy, it allows you to conduct true correlative analysis.

Rheonaut Module (FTIR) for HAAKE MARS Rheometers

The Thermo Scientific Rheonaut Module with the Thermo Scientific HAAKE MARS Rheometer Platform simultaneously measures rheological properties and structural changes on the molecular level using FT-IR spectroscopy. The combined analysis allows extensive investigations of structural changes under deformation/shear as well as thermally induced or UV curing. Understanding rheological phenomena on the molecular level enables researchers to speed up formulation development and process optimization.

Advanced multi-modal analysis technologies

Raman spectroscopy

Raman spectroscopy is an analytical technique that observes vibrational, rotational, and other low-frequency modes in a system through inelastic scattering of monochromatic light, usually from a laser. This interaction shifts the energy of the laser photons, revealing information about molecular vibrations. It is valuable for characterizing molecular structures, identifying substances, and studying molecular interactions without extensive sample preparation.

FTIR spectroscopy

FTIR stands for Fourier transform infrared, the preferred method of infrared spectroscopy. When IR radiation is passed through a sample, some radiation is absorbed by the sample and some passes through (is transmitted). The resulting signal at the detector is a spectrum representing a molecular ‘fingerprint’ of the sample. The usefulness of infrared spectroscopy arises because different chemical structures (molecules) produce different spectral fingerprints

X-Ray photoelectron spectroscopy (XPS)

X-ray photoelectron spectroscopy, also known as electron spectroscopy for chemical analysis (ESCA), is a highly surface-sensitive, quantitative, chemical analysis technique that can be used to solve a wide range of materials problems. XPS is the measurement of photoelectrons ejected from the surface of a material that has been irradiated with X-rays. The kinetic energy of the emitted photoelectrons is measured. This energy is directly related to the photoelectrons’ binding energy within the parent atom and is characteristic of the element and its chemical state.

Compounding & extrusion, rheology

Compounding & extrusion and rheology are essential in industrial ceramics and glass manufacturing. Compounding involves mixing raw materials to create a homogeneous mixture, while extrusion shapes this mixture into desired forms. Rheology studies the flow behavior of these materials, helping optimize processes like mixing and molding, and ensuring quality control. Together, these techniques are used to analyze the material and help ensure efficient production and high-quality, consistent products.

Featured resources

Technique

Asset type

Asset title

FTIR, Thermal Gravimetric Analysis (TGA)

Application Note

Doing the Dirty Work: Combined TGA-IR and Transmission Studies of Soil

FTIR, Thermal Gravimetric Analysis (TGA)

Application Note

Complete Materials Deformulation Using TGA-IR

FTIR, Thermal Gravimetric Analysis (TGA)

Application Note

TGA-IR Analysis Using the OMNIC Mercury TGA

FTIR, Thermal Gravimetric Analysis (TGA)

Specification Sheet

TGA-IR Module for Nicolet FTIR Spectrometers

FTIR, Raman

Poster Note

Complementary Use of Raman and FTIR Imaging for the Analysis of Multi-Layer Polymer Composites

FTIR, Raman

Webinar

Rheometry & FTIR Spectroscopy: Benefits & Applications in Polymer Research

FTIR, Raman

Webinar

Peeling Back the Layers – Characterizing Multi-layer Structures using FTIR and Raman Microscopy

FTIR, Rheology

Application Note

Detailed Analysis of Curing Reactions of Polyurethane Resins Using the Rheonaut technology for Simultaneous Rheometry and FTIR

FTIR, Rheology

Application Note

Investigating heat-induced gelation of whey protein using simultaneous rheology and FTIR spectroscopy

FTIR, Rheology

Webinar

Rheo-Kinetic Study of Thermoplastic Polyurethanes Using in-situ Rheo-FTIR

Raman, Rheology

Specification Sheet

HAAKE MARS Rheo-Raman System

Raman

Specification Sheet

DXR3 Flex Raman Spectrometer

Raman, Rheology

Application Note

Rheology-Raman Spectroscopy: Tracking Polymer Crystallization with the Combination of a Rheometer and a Raman Microscope

Raman, Rheology

Application Note

Rheology-Raman Spectroscopy: Tracking Emulsion Stability with the Combination of a Rheometer and a Raman Microscope

Raman, Rheology

Application Note

Simultaneous Rheology and Raman Spectroscopy During the Melting and Recrystallization of Polypropylene

Raman, Rheology

Poster Note

Rheology-Raman Spectroscopy: Tracking Molecular Structures as a Function of Deformation and Temperature

Raman, Rheology

Specification Sheet

HAAKE MARS XR RheoRaman System

Raman, Rheology

Webinar

Benefits of Combining Rheometry with Raman Spectroscopy for Materials Science

Raman, Rheology

Webinar

The Rheo-Raman Microscope: Simultaneous Measures of Soft Materials

Raman, Rheology

Application Note

Tracking Crystallization of EVA/Acetaminophen Mixtures with Rheo-Raman Analysis

Raman, Rheology

Application Note

Rheology-Raman spectroscopy during the melting and recrystallization of polypropylene

Raman, XPS

Poster Note

Using Raman and XPS in the Development of Graphene-based Materials

SEM, EDS

Webinar

Feature Sizing - Sparse Particle-Inclusion Analysis

SEM, TEM

Webinar

Introduction to DualBeam FIB-SEM for S/TEM Sample Preparation

XPS, UPS

Webinar

Enhance XPS Surface Analysis Capabilities with UV Photoelectron Spectroscopy

For Research Use Only. Not for use in diagnostic procedures.